| 1,1'-Bi-2-naphthol |
 |
| Column: |
YMC Chiral NEA (R) 250 x 4.6 mm i.d. |
| Eluent: |
Acetonitrile/Water (50/50) |
| Flow: |
1.0 ml/min |
| Pressure: |
80 bar |
| Detection: |
UV at 235 nm |
| Injection: |
1.0 μl (2.8 mg/ml) |
| Temperature |
ambient |
|
|
|
|
|
| Propranolol · HCl |
 |
| Column: |
YMC Chiral NEA (R) 250 x 4.6 mm i.d. |
| a) |
|
| Eluent: |
Acetonitrile/NaClO4 0.5M (40/60) |
| Flow: |
1.0 ml/min |
| Temperature: |
ambient |
| Time: |
100 hours |
| b) |
|
| Eluent: |
Acetonitrile/NaClO4 0.5M (40/60) |
| Flow: |
1.0 ml/min |
| Temperature: |
ambient |
| Detection: |
UV at 254 nm |
|
|
| |
|
|
| Hexobarbital |
 |
| Column: |
YMC Chiral NEA (R) 250 x 4.6 mm i.d. |
| Eluent: |
Acetonitrile/Water (30/70) |
| Flow: |
0.7 ml/min |
| Pressure: |
80 bar |
| Detection: |
UV at 210 nm |
| Injection: |
1.0 μl (1.2 mg/ml) |
| Temperature |
ambient |
|
|
|
| Ketamin · HCl |
 |
| Column: |
YMC Chiral NEA (R) 250 x 4.6 mm i.d. |
| Eluent: |
Acetonitrile/NaClO4 0.5M (40/60) |
| Flow: |
1.0 ml/min |
| Pressure: |
85 bar |
| Detection: |
UV at 268 nm |
| Injection: |
10 μl (1.4 mg/ml) |
| Temperature |
ambient |
|
|
| |
|
|
| 2,2,2-Trifluoro-1-(9-anthryl)-ethanol |
 |
| Column: |
YMC Chiral NEA (R) 250 x 4.6 mm i.d. |
| Eluent: |
Acetonitrile/Water (40/60) |
| Flow: |
1.0 ml/min |
| Pressure: |
85 bar |
| Detection: |
UV at 254 nm |
| Injection: |
1.0 μl (0.14 mg/ml) |
| Temperature |
ambient |
|
|
|
| CBZ-Phenylalanine (Z-Phe-OH) |
 |
| Column: |
YMC Chiral NEA (R) 250 x 4.6 mm i.d. |
| Eluent: |
0.5M NaClO4-HClO4 (pH 2.0) / Acetonitrile (70/30) |
| Flow: |
1.0 ml/min |
| Pressure: |
100 bar |
| Detection: |
UV at 254 nm |
| Injection: |
10 μl (1.5 mg/ml) |
| Temperature |
ambient |
|
|
Start
