| Steroids from toad venom |
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Column:
Eluent:
Flow:
Detection:
Temperature:
Injection: |
YMC-Pack ODS-AL (5 μm, 12 nm) 150 x 4.6 mm i.d.
ACN / 0.1% phosphoric acid (45/55)
1.0 ml/min
UV at 300 nm, 0.08 AUFS
40 °C
10 μl (0.04 ~ 0.08 mg/ml)
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| Disinfectants |
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Column:
Eluent:
Flow:
Detection:
Temperature:
Injection: |
YMC-Pack ODS-AL (5 μm, 12 nm) 150 x 4.6 mm i.d.
100 mM KH2PO4-K2HPO4 (pH 7.0) / methanol (75/25)
0.8 ml/min
UV at 270 nm, 0.13 AUFS
30 °C
3 μl (0.1 ~ 0.8 mg/ml)
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| Sterols |
|
Column:
Eluent:
Flow:
Detection:
Temperature:
Injection: |
YMC-Pack ODS-AL (5 μm, 12 nm) 150 x 4.6 mm i.d.
methanol / water (100/2)
0.8 ml/min
UV at 210 nm, 0.32 AUFS
40 °C
10 μl (0.4 ~ 1 mg/ml)
|
| Vitamin D2 and Vitamin D3 |
|
Column:
Eluent:
Flow:
Detection:
Temperature:
Injection: |
YMC-Pack ODS-AL (5 μm, 12 nm) 150 x 4.6 mm i.d.
acetonitrile / water (95/5)
1.0 ml/min
UV at 265 nm
40 °C
10 μl (0.01 mg/ml)
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